Changes

no edit summary
Line 48: Line 48:  
'''conventional hydrocarbons'''<br>
 
'''conventional hydrocarbons'''<br>
 
petroleum-derived hydrocarbons from natural gas liquid condensates, crude oil, heavy oil, shale oil and oil sands, which are generally accompanied by lower levels of naturally occurring non-hydrocarbons.<br>
 
petroleum-derived hydrocarbons from natural gas liquid condensates, crude oil, heavy oil, shale oil and oil sands, which are generally accompanied by lower levels of naturally occurring non-hydrocarbons.<br>
''3.2'''<br>
+
 
 +
''3.2''<br>
 
'''operability temperature'''<br>
 
'''operability temperature'''<br>
 
lowest temperature at which the fuel oil is designed to provide satisfactory performance under the conditions of storage and use (see 6.23, 6.24 and 9.2).The 2.5 percentile low-end design temperature  is the temperature at or below which 2.5% of the hourly outside air temperatures are observed to occur for an indicated half month. The 2.5% low-end design temperature for most weather stations in Canada by half month period is available on the Canadian Fuels Association Web site (see 2.2). This data is based upon a statistical analysis of hourly weather readings from weather stations across Canada over the thirty year period from 1981 to 2010 inclusive.
 
lowest temperature at which the fuel oil is designed to provide satisfactory performance under the conditions of storage and use (see 6.23, 6.24 and 9.2).The 2.5 percentile low-end design temperature  is the temperature at or below which 2.5% of the hourly outside air temperatures are observed to occur for an indicated half month. The 2.5% low-end design temperature for most weather stations in Canada by half month period is available on the Canadian Fuels Association Web site (see 2.2). This data is based upon a statistical analysis of hourly weather readings from weather stations across Canada over the thirty year period from 1981 to 2010 inclusive.
Line 64: Line 65:  
Heating fuel oils shall be supplied in the following types, as specified (see 8.1):<br>
 
Heating fuel oils shall be supplied in the following types, as specified (see 8.1):<br>
   −
4.1.1 Types<br>
+
4.1.1 Types<br>
Type 0<br>
+
:Type 0<br>
Type 1<br>
+
:Type 1<br>
Type 2<br>
+
:Type 2<br>
Type 4<br>
+
:Type 4<br>
Type 5<br>
+
:Type 5<br>
Type 6
+
:Type 6
    
<h2> General requirements </h2>
 
<h2> General requirements </h2>
'''5.1 '''Unless otherwise allowed (see 5.4 and 6.17), the heating fuel oils shall consist of conventional hydrocarbons (i.e. petroleum-derived from natural gas liquid condensates, crude oil, heavy oil, shale oil and oil sands), synthetic hydrocarbons (see 9.13) or mixtures of conventional and synthetic hydrocarbons and may include naturally occurring non-hydrocarbons.  <br>
+
'''5.1''' Unless otherwise allowed (see 5.4 and 6.17), the heating fuel oils shall consist of conventional hydrocarbons (i.e. petroleum-derived from natural gas liquid condensates, crude oil, heavy oil, shale oil and oil sands), synthetic hydrocarbons (see 9.13) or mixtures of conventional and synthetic hydrocarbons and may include naturally occurring non-hydrocarbons.  <br>
'''5.2 '''The heating fuel oils may contain additives designed to improve the characteristics or performance of the fuel oil. Additives include those that enhance low-temperature flow properties, storage life, static charge dissipation, water haze dissipation, lubricity and inhibit corrosion.<br>
+
'''5.2''' The heating fuel oils may contain additives designed to improve the characteristics or performance of the fuel oil. Additives include those that enhance low-temperature flow properties, storage life, static charge dissipation, water haze dissipation, lubricity and inhibit corrosion.<br>
'''5.3 '''The heating fuel oils shall be a stable homogeneous liquid, free of foreign matter that is likely to clog filters or nozzles, or to damage equipment.<br>
+
'''5.3''' The heating fuel oils shall be a stable homogeneous liquid, free of foreign matter that is likely to clog filters or nozzles, or to damage equipment.<br>
'''5.4 '''In Types 0, 1 and 2 fuel oils, there shall be no intentional addition of used lubricating oils, used solvents, triglycerides (such as raw vegetable oils, animal fats, fish oils or used cooking oils), or other fluids which are not normal components of the fuel. Types 4, 5 and 6 fuel oils may contain used lubricating oils or other fluids provided that the fuel oil is used in specifically designed equipment and the relevant authority approves their use.<br>
+
'''5.4''' In Types 0, 1 and 2 fuel oils, there shall be no intentional addition of used lubricating oils, used solvents, triglycerides (such as raw vegetable oils, animal fats, fish oils or used cooking oils), or other fluids which are not normal components of the fuel. Types 4, 5 and 6 fuel oils may contain used lubricating oils or other fluids provided that the fuel oil is used in specifically designed equipment and the relevant authority approves their use.<br>
'''5.5 '''The heating fuel oils shall remain undyed except when it is required for taxation purposes by provincial or territorial regulation.
+
'''5.5''' The heating fuel oils shall remain undyed except when it is required for taxation purposes by provincial or territorial regulation.
    
<h2> Detailed requirements </h2>
 
<h2> Detailed requirements </h2>
 
<h3> Specified limiting values </h3>
 
<h3> Specified limiting values </h3>
 
'''6.1.1''' The heating fuel oil shall comply with the specified limiting values. The specified limiting values shall not be changed. This precludes any allowances for the test method precision and for adding or subtracting digits.<br>
 
'''6.1.1''' The heating fuel oil shall comply with the specified limiting values. The specified limiting values shall not be changed. This precludes any allowances for the test method precision and for adding or subtracting digits.<br>
'''6.1.2''' For purposes of determining conformance with the specified limiting values, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specified limiting value, in accordance with the rounding-off method of ASTM E29. There are two exceptions (see 6.3 and 6.17).<br>
+
'''6.1.2''' For purposes of determining conformance with the specified limiting values, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specified limiting value, in accordance with the rounding-off method of [https://www.astm.org/Standards/E29.htm ASTM E29]. There are two exceptions (see 6.3 and 6.17).<br>
 
'''6.1.3''' If an alternate test method referenced in this standard provides a bias correction to the referee method, adherence to the specified limiting value shall be based on the bias-corrected result.<br>
 
'''6.1.3''' If an alternate test method referenced in this standard provides a bias correction to the referee method, adherence to the specified limiting value shall be based on the bias-corrected result.<br>
'''6.1.4''' Where test values differ between two parties, a resolution shall be in accordance with ASTM D3244 in order to determine conformance with the specified limiting values, with the criticality of the limits set at P = 0.5.<br>
+
'''6.1.4''' Where test values differ between two parties, a resolution shall be in accordance with [https://www.astm.org/Standards/D3244.htm ASTM 3244] in order to determine conformance with the specified limiting values, with the criticality of the limits set at P = 0.5.<br>
'''6.1.5''' Zeroes trailing the last nonzero digit for numbers represented with a decimal point are significant digits, in accordance with ASTM E29.
+
'''6.1.5''' Zeroes trailing the last nonzero digit for numbers represented with a decimal point are significant digits, in accordance with [https://www.astm.org/Standards/E29.htm ASTM E29].
 
<h3> Test methods </h3>
 
<h3> Test methods </h3>
 
'''6.2.1''' Test methods other than those referenced in this standard may be used only if they have been validated in accordance with ASTM D3764 or D6708.<br>
 
'''6.2.1''' Test methods other than those referenced in this standard may be used only if they have been validated in accordance with ASTM D3764 or D6708.<br>
Line 99: Line 100:  
! # !! Property !! Limit !! Type 0 !! Type 1 !! Type 2 !! Type 4 !! Type 5 !! Type 6 !! Test Method (ASTM)
 
! # !! Property !! Limit !! Type 0 !! Type 1 !! Type 2 !! Type 4 !! Type 5 !! Type 6 !! Test Method (ASTM)
 
|-
 
|-
| '''6.3''' || Flash point, °C (see 6.19) || Min. || 40.0 || 40.0 || 40.0 || 54.0 || 54.0 || 60.0 || D93<sup>[[CGSB_ONGC/003_0002_2019_ENG#Normative_a|a]] </sup>, D3828, D7049  
+
| '''6.3''' || Flash point, °C (see 6.19) || Min. || 40.0 || 40.0 || 40.0 || 54.0 || 54.0 || 60.0 || D93<ref name="a">The referee method to be used in the event of a dispute.</ref>, D3828<ref name="b">The results obtained by ASTM D3828 can be more than 2°C lower than those obtained by ASTM D93, the referee method.</ref>, D7049  
 
|-
 
|-
| '''6.4''' || Kinematic viscosity, at 40°C, mm<sup>2</sup>/s (cSt)(see 6.25) || Min. || 1.20 || 1.30 || 1.70 || 5.5 || ― || ― ||D445 a<ref>The referee method to be used in the event of a dispute</ref> , D7042 or D7945  
+
| '''6.4''' Min. || Kinematic viscosity, at 40°C, mm<sup>2</sup>/s (cSt)<ref name="c">The SI unit for kinematic viscosity is the square metre per second. The preferred multiple for fluids in this viscosity range is the square millimetre per second, which is equivalent to a centiStokes (i.e. 1 mm<sup>2</sup>/s = 1 cSt).</ref> (see 6.25) || Min. || 1.20 || 1.30 || 1.70 || 5.5 || ― || ― ||D445<ref name="a">The referee method to be used in the event of a dispute.</ref>, D7042 or D7945  
 
|-
 
|-
| || || Max. || 2.00 || 2.50 || 3.60 || 24.0 || ― || ―
+
| '''6.4''' Max. || Kinematic viscosity, at 40°C, mm<sup>2</sup>/s (cSt)(see 6.25) || Max. || 2.00 || 2.50 || 3.60 || 24.0 || ― || ―
 
|-
 
|-
| '''6.5''' || Kinematic viscosity, at 50°C, mm2/s (cSt) || Min. || ― || ― || ― || ― || 15 || 100. || D445 or D702
+
| '''6.5''' Min. || Kinematic viscosity, at 50°C, mm<sup>2</sup>/s (cSt) || Min. || ― || ― || ― || ― || 15 || 100. || D445<ref name="a">The referee method to be used in the event of a dispute.</ref> or D7042
 
|-
 
|-
| '''6.6''' || Distillation (see 6.20) ||  ||  ||  ||  ||  ||  ||  || D86, D2887, or D7345
+
| '''6.5''' Max. ||Kinematic viscosity, at 50°C, mm<sup>2</sup>/s (cSt) || Max. || ― || ― || ― || ― || 100. || 650. ||
 +
|-
 +
| '''6.6''' || Distillation (see 6.20) ||  ||  ||  ||  ||  ||  ||  || D86<ref name="a">The referee method to be used in the event of a dispute.</ref>, D2887, or D7345
 
|-
 
|-
 
| 6.6 a || 10% recovered, °C || Max. || ― || 215 || ― || ― || ― || ― ||  
 
| 6.6 a || 10% recovered, °C || Max. || ― || 215 || ― || ― || ― || ― ||  
Line 115: Line 118:  
| 6.6 c || end point, °C  || Max. || 300. || ― || ― || ― || ― || ― ||   
 
| 6.6 c || end point, °C  || Max. || 300. || ― || ― || ― || ― || ― ||   
 
|-
 
|-
| Example || Example || Example || Example || Example || Example || Example || Example || Example
+
| '''6.7'''  || Water and sediment, % by volume (see 6.21) || Max. || 0.02 || 0.02 || 0.02 || || || ― || D1796 <ref name="a">The referee method to be used in the event of a dispute.</ref>,(modified) or D2709
 +
|-
 +
| || || Max. || ― || ― || ― || 0.50 || 1.00|| 1.00 || D95<ref name="a">The referee method to be used in the event of a dispute.</ref>,  and D473
 +
|-
 +
| '''6.8''' || Sulphur, % by mass (see 6.22 and 8.2) || Max. || 0.30 || 0.30 || 0.50 || ― || ― || ― || D1266, D1552, D2622, D4294, D5453<ref name="a">The referee method to be used in the event of a dispute.</ref>,  or D7039
 +
|-
 +
| '''6.9''' || Copper strip corrosion, 3 h at minimum test temperature of 50°C h (see 9.4) || Max. || No. 1 || No. 1 || No.1 || ― || ― || ― || D130
 +
|-
 +
| '''6.10''' || Carbon residue on 10% bottoms, % by mass  || Max. || 0.1 || 0.1 || 0.3 || ― || ― || ― || D524 or D4530<ref name="a">The referee method to be used in the event of a dispute.</ref>,
 +
|-
 +
| '''6.11''' || Ash, % by mass  || Max. || 0.010 || 0.010 || 0.010 || 0.10 || 0.10 || 0.20 || D482
 +
|-
 +
| '''6.12'''  || Electrical conductivity, at point, time, and temperature of delivery to purchaser, pS/m (see 9.5) || Min. || 25 || 25 || 25 || ― || ― || ― || D2624
 +
|-
 +
| '''6.13''' || Density, at 15°C, kg/m3 (kg/L ) || Max. || 840. (0.840) || 850. (0.850)|| 900. (0.900)|| ― || ― || ― ||  D1298, D4052<ref name="a">The referee method to be used in the event of a dispute.</ref>, D7042
 +
|-
 +
| '''6.14''' || Total sediment, % by mass || Max. || ― || ― || ― || 0.10 || 0.15 || 0.20 || D4870
 +
|-
 +
| '''6.15''' || Pour point, °C(see 6.23, 8.1 and 9.2) || Max. ||  -48  ||  Report  ||  Report ||  ―  ||  ―  ||  ―  || D97 or D5949<ref name="a">The referee method to be used in the event of a dispute.</ref>, 
 +
|-
 +
| || || Max. || ― || ― || ― || Report || ― || ― || D97
 
|-
 
|-
| Example || Example || Example || Example || Example || Example || Example || Example || Example
+
| '''6.16''' || Cloud point, °C (see 6.24 and 8.1) || Max. || -48 || Report || Report || ―  || ―  || ―  || D2500 and D5773<ref name="a">The referee method to be used in the event of a dispute.</ref>,
 
|-
 
|-
| Example || Example || Example || Example || Example || Example || Example || Example || Example
+
| '''6.17''' Min. || Biodiesel, % by volume see 6.25 and Annex C) || Min. || ―  || ―  || ―  || ―  || ―  || ―  || D7371<ref name="a">The referee method to be used in the event of a dispute.</ref>,  or D7806
 
|-
 
|-
| Example || Example || Example || Example || Example || Example || Example || Example || Example
+
| '''6.17''' Max. || Biodiesel, % by volume see 6.25 and Annex C)  || Max. || 0 || 0 || 5 || ―  || ―  || ―  || D7371<ref name="a">The referee method to be used in the event of a dispute.</ref>,  or D7806
 
|-
 
|-
| Example || Example || Example || Example || Example || Example || Example || Example || Example
+
| '''6.18''' || Lubricity, micrometers, µm (see 9.13)|| Max. || 520. || 520. || 520. || || || ― || D6079<ref name="a">The referee method to be used in the event of a dispute.</ref>,  or D7688
 
|}
 
|}
 
<references> Normative References in Specified Values </references>
 
<references> Normative References in Specified Values </references>
Line 134: Line 157:  
'''Annual Book of ASTM Standards'''<br>
 
'''Annual Book of ASTM Standards'''<br>
 
[https://www.astm.org/Standards/D86.htm D86 Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure]<br>
 
[https://www.astm.org/Standards/D86.htm D86 Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure]<br>
D93 Standard Test Methods for Flash Point by Pensky-Martens Closed Cup Tester<br>
+
[https://www.astm.org/Standards/D93.htm D93 Standard Test Methods for Flash Point by Pensky-Martens Closed Cup Tester]<br>
 
D95 Standard Test Method for Water in Petroleum Products and Bituminous Materials by Distillation<br>
 
D95 Standard Test Method for Water in Petroleum Products and Bituminous Materials by Distillation<br>
 
D97 Standard Test Method for Pour Point of Petroleum Products<br>
 
D97 Standard Test Method for Pour Point of Petroleum Products<br>
Line 238: Line 261:     
by e-mail — ncr.cgsb-ongc@tpsgc-pwgsc.gc.ca<br>
 
by e-mail — ncr.cgsb-ongc@tpsgc-pwgsc.gc.ca<br>
on the Web — www.tpsgc-pwgsc.gc.ca/ongc-cgsb <br>
+
on the Web — http://www.tpsgc-pwgsc.gc.ca/ongc-cgsb <br>