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| <h2> '''6. Detailed requirements''' </h2> | | <h2> '''6. Detailed requirements''' </h2> |
− | <h3> Specified limiting values </h3> | + | <h5> 6.1 Specified limiting values </h5> |
− | <h5>'''6.1.1'''</h5> The heating fuel oil shall comply with the specified limiting values. The specified limiting values shall not be changed. This precludes any allowances for the test method precision and for adding or subtracting digits.<br>
| + | '''6.1.1''' The heating fuel oil shall comply with the specified limiting values. The specified limiting values shall not be changed. This precludes any allowances for the test method precision and for adding or subtracting digits.<br> |
| '''6.1.2''' For purposes of determining conformance with the specified limiting values, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specified limiting value, in accordance with the rounding-off method of [https://www.astm.org/Standards/E29.htm ASTM E29]. There are two exceptions (see [[6.3]] and 6.17).<br> | | '''6.1.2''' For purposes of determining conformance with the specified limiting values, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specified limiting value, in accordance with the rounding-off method of [https://www.astm.org/Standards/E29.htm ASTM E29]. There are two exceptions (see [[6.3]] and 6.17).<br> |
| '''6.1.3''' If an alternate test method referenced in this standard provides a bias correction to the referee method, adherence to the specified limiting value shall be based on the bias-corrected result.<br> | | '''6.1.3''' If an alternate test method referenced in this standard provides a bias correction to the referee method, adherence to the specified limiting value shall be based on the bias-corrected result.<br> |
| '''6.1.4''' Where test values differ between two parties, a resolution shall be in accordance with [https://www.astm.org/Standards/D3244.htm ASTM 3244] in order to determine conformance with the specified limiting values, with the criticality of the limits set at P = 0.5.<br> | | '''6.1.4''' Where test values differ between two parties, a resolution shall be in accordance with [https://www.astm.org/Standards/D3244.htm ASTM 3244] in order to determine conformance with the specified limiting values, with the criticality of the limits set at P = 0.5.<br> |
| '''6.1.5''' Zeroes trailing the last nonzero digit for numbers represented with a decimal point are significant digits, in accordance with [https://www.astm.org/Standards/E29.htm ASTM E29]. | | '''6.1.5''' Zeroes trailing the last nonzero digit for numbers represented with a decimal point are significant digits, in accordance with [https://www.astm.org/Standards/E29.htm ASTM E29]. |
− | <h3> Test methods </h3> | + | <h5> 6.2 Test methods </h5> |
| '''6.2.1''' Test methods other than those referenced in this standard may be used only if they have been validated in accordance with ASTM D3764 or D6708.<br> | | '''6.2.1''' Test methods other than those referenced in this standard may be used only if they have been validated in accordance with ASTM D3764 or D6708.<br> |
| '''6.2.2''' Validated test methods shall correlate with methods referenced in the standard. Differences in precision, sensitivity and bias between methods referenced in the standard and the validated methods shall be noted when using results from validated methods.<br> | | '''6.2.2''' Validated test methods shall correlate with methods referenced in the standard. Differences in precision, sensitivity and bias between methods referenced in the standard and the validated methods shall be noted when using results from validated methods.<br> |
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| {| class="wikitable" | | {| class="wikitable" |
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− | ! colspan="10" | Specified limiting values | + | ! colspan="10" | Table of Specified limiting values |
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| ! # !! Property !! Limit !! Type 0 !! Type 1 !! Type 2 !! Type 4 !! Type 5 !! Type 6 !! Test Method (ASTM) | | ! # !! Property !! Limit !! Type 0 !! Type 1 !! Type 2 !! Type 4 !! Type 5 !! Type 6 !! Test Method (ASTM) |
| |- | | |- |
− | | '''6.3''' || Flash point, °C (see 6.19) || Min. || 40.0 || 40.0 || 40.0 || 54.0 || 54.0 || 60.0 || D93<ref name="a">The referee method to be used in the event of a dispute.</ref>, D3828<ref name="b">The results obtained by ASTM D3828 can be more than 2°C lower than those obtained by ASTM D93, the referee method.</ref>, D7049 | + | | <h5>'''6.3'''</h5> || Flash point, °C (see 6.19) || Min. || 40.0 || 40.0 || 40.0 || 54.0 || 54.0 || 60.0 || D93<ref name="a">The referee method to be used in the event of a dispute.</ref>, D3828<ref name="b">The results obtained by ASTM D3828 can be more than 2°C lower than those obtained by ASTM D93, the referee method.</ref>, D7049 |
| |- | | |- |
| | '''6.4''' <abbr title="Minimum"> Min. </abbr> || Kinematic viscosity, at 40°C, mm<sup>2</sup>/s (cSt)<ref name="c">The SI unit for kinematic viscosity is the square metre per second. The preferred multiple for fluids in this viscosity range is the square millimetre per second, which is equivalent to a centiStokes (i.e. 1 mm<sup>2</sup>/s = 1 cSt).</ref> (see 6.25) || Min. || 1.20 || 1.30 || 1.70 || 5.5 || ― || ― ||D445<ref name="a">The referee method to be used in the event of a dispute.</ref>, D7042 or D7945 | | | '''6.4''' <abbr title="Minimum"> Min. </abbr> || Kinematic viscosity, at 40°C, mm<sup>2</sup>/s (cSt)<ref name="c">The SI unit for kinematic viscosity is the square metre per second. The preferred multiple for fluids in this viscosity range is the square millimetre per second, which is equivalent to a centiStokes (i.e. 1 mm<sup>2</sup>/s = 1 cSt).</ref> (see 6.25) || Min. || 1.20 || 1.30 || 1.70 || 5.5 || ― || ― ||D445<ref name="a">The referee method to be used in the event of a dispute.</ref>, D7042 or D7945 |
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− | | '''6.4''' Max. || Kinematic viscosity, at 40°C, mm<sup>2</sup>/s (cSt)(see 6.25) || Max. || 2.00 || 2.50 || 3.60 || 24.0 || ― || ― | + | | '''6.4''' Max. || Kinematic viscosity, at 40°C, mm<sup>2</sup>/s (cSt)(see 6.25) || Max. || 2.00 || 2.50 || 3.60 || 24.0 || ― || ― || ― |
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| | '''6.5''' Min. || Kinematic viscosity, at 50°C, mm<sup>2</sup>/s (cSt) || Min. || ― || ― || ― || ― || 15 || 100. || D445<ref name="a">The referee method to be used in the event of a dispute.</ref> or D7042 | | | '''6.5''' Min. || Kinematic viscosity, at 50°C, mm<sup>2</sup>/s (cSt) || Min. || ― || ― || ― || ― || 15 || 100. || D445<ref name="a">The referee method to be used in the event of a dispute.</ref> or D7042 |